ZnO基氯气传感元件的制备及其气敏性能
Preparation and sensitive characteristics of ZnO-based chlorine gas sensor
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摘要: 以硝酸锌和氨水为反应物,采用沉淀法制备ZnO纳米粉体。通过X射线衍射仪和透射电镜对其进行分析,结果表明,制得的ZnO颗粒为球形,粒径较小,在20nm左右,为六方形纤锌矿结构。通过掺杂In2O3,大大提高元件对氯气的气敏特性。实验表明,该元件对体积分数为20×10-6的氯气,灵敏度可达301,响应时间2秒,恢复时间在110秒左右,具有高选择性。Abstract: The ZnO nanoparticles,prepared from zinc nitrate and ammonia by deposition method,are analysed through the X-ray diffraction and TEM.The results show that the particles are global,very small(about 20 nm in size) and assigned to the hexagonal zincite-structure.The gas sensitive properties to chlorine gas are improved greatly by doping In2O3.The experiments show that the sensitivity of the component to 20×10-6(volume percentage)chlorine gas is up to 301,the response time is 2 seconds,and the recovery time is about 110 seconds with high selectivity.
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