Abstract: The technology research on manganese zinc ferrite preparation progress was reviewed,mainly including the traditional solid method,the chemical co-precipitation method,the hydrothermal technique,the sol-gel method and auto-combustion method. The principle and applications of these methods have been discussed,the advantages and drawbacks have been analyzed. Among these,the chemical co-precipitation method,the sol-gel auto-combustion method have been widely used. The hydrothermal technique and microemulsion method have important applications in the preparation of nanometer manganese zinc ferrite crystal and related functional materials. The analysis shows that the manganese zinc ferrite preparation needs to be further improved. The manganese zinc ferrite and conductive polymer composites,preparation manganese zinc ferrite with the external magnetic field? shall be further investigated in future.