玻璃包覆Fe79-xCoxSi8B13非晶合金微丝的磁性能

Magnetic properties of glass-coated amorphous Fe79-xCoxSi8B13 microwires

  • 摘要: 实验以熔融纺丝法制备的玻璃包覆Fe79-xCoxSi8B13非晶合金微丝为对象,分析了微丝成分、尺寸以及玻璃包覆层去除对微丝静磁性能的影响。研究结果表明,玻璃包覆Fe79-xCoxSi8B13非晶合金微丝存在明显的磁各向异性,微丝轴向为易磁化方向;随着Co含量的增加,微丝的饱和磁化强度先增大后减小,Co含量为10%的Fe69Co10Si8B13非晶合金微丝饱和磁化强度最高,为1323emu·cm-3;对于玻璃包覆Fe69Co10Si8B13非晶合金微丝,当芯丝半径与玻璃包覆层厚度比值k约小于0.5时,其轴向磁滞回线为近矩形,表现出大巴克豪森效应;微丝的轴向剩磁比随k值的增大而减小,而微丝径向剩磁比保持很小,仅0.03左右;微丝的轴向和径向矫顽力均随比值k的增大而减小;当芯丝半径为10.9μm、玻璃包覆层厚度为9.7μm(k为1.12)时,去除包覆层后微丝的轴向矫顽力降低30%、径向矫顽力降低11%;而轴向剩磁比降低33%、径向剩磁比降低67%。

     

    Abstract: The influences of alloy composition,geometrical characteristics and glass coating on the magnetic properties of the glass-coated amorphous Fe79-xCoxSi8B13 microwires are investigated. The results show that the glass-coated amorphous Fe79-xCoxSi8B13 microwires exhibit obvious magnetic anisotropy and the direction of easy magnetization is the axial direction. With cobalt content increasing,the saturation magnetization of the glass-coated amorphous Fe79-xCoxSi8B13 microwires increases firstly and then decreases. When the cobalt content is 10%,the saturation magnetization of the microwire achieves maximum value,being 1323emu·cm-3. As the glass-coated amorphous Fe69Co10Si8B13 microwire,when the ratio k of metal core radius and glass coating thickness is less than 0.5,the axial hysteresis loop of the microwire is rectangular and appears large Barkhausen effect. With the kincreasing,the axial remanence ratio of the microwire decreases,but the radial remanence ratio keeps very small (about 0.03). Both the axial and radial coercivities of the microwires decrease with kincreasing. After removing the glass coating,the axial and radial coercivities of the microwire with the initial glass coating thickness of 9.7μm and metal core radius of 10.9μm decrease 30% and 11%,respectively. Meanwhile,the axial and radial remanence ratios decrease 33% and 67%,respectively.

     

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