玻璃上低温沉积碳纳米管薄膜及其场发射研究

The carbon nanotube films study growth mechanism on glass and field emission properties

  • 摘要: 本文从事的研究是碳纳米管(CNT)薄膜的制备及场发射效果分析。在普通玻璃衬底上用磁控溅射方法镀上金属钛层,用含铁杂质的碳化硅微粒对钛层进行抛光。利用微波等离子体化学气相沉积法,在小于500℃衬底温度下快速制备出CNT膜。通过扫描电子显微镜、拉曼光谱,分析了薄膜的表面形貌和结构特性。通过二级管结构测试了聚晶膜的场致电子发射特性,对于制备的碳膜,在电场时,最大场发射电流密度达。并对其发射机理进行了研究。

     

    Abstract: This study is the carbon nanotube films(CNT)in the Preparation and Field Emission Effect.The carbon nanotubefilms were fabricated in 500℃ temperature by microwave plasma chemical vapor deposition(MPCVD) method.The glass with a Ti mental layer was used as substrate.Before fabricating,the substrate was polling by the SiO2 with Fe.The CNT films were evaluated by Raman scattering spectroscopy,scanning electron microscopy(SEM) and Transmission electron microscope(TEM).The field emission properties were tested by using a diode structure in a vacuum.A phosphor-coated indium tin oxide(ITO) anode was used for observing and characterizing the field emission.It was found that CNT films exhibited good electron emission properties.The turn-on field was only 1.1V/μm and the emission current density as high as 9.0mA/cm2 was obtained under an applied field of 3.0V/μm for the last operation.The growth mechanism and field emission properties of the CNT films are discussed relating to microstructure and electrical conductivity.

     

/

返回文章
返回