Al2O3透明陶瓷显微结构的研究

Characterization of transparent Al2O3 ceramics microstructure

  • 摘要: 采用高纯Al2O3(>99.9%)粉末为原料,用无压烧结工艺制备Al2O3透明陶瓷。研究了添加剂Y2O3、烧结温度、保温时间等对Al2O3透明陶瓷显微结构和光学性能的影响。实验结果表明,适量的Y2O3能够抑制Al2O3晶粒的生长,改善烧结性能,但添加量过多会使Al2O3陶瓷气孔略有增加。在1800℃烧结的样品密度接近理论密度,具有较好的光学性能。延长保温时间能够使晶粒长大的同时有效排除晶界处少量气孔。

     

    Abstract: Optical transparent polycrystalline Al2O3 ceramics were fabricated by conventional solid-state pressureless sintering processing using high-purity powder of Al2O3(>99.9wt%purity). The effects of Y2O3 additive, sintering temperature and sintering holding time on the microstructure and optical properties of Al2O3 were investigated. The results indicate that small amounts of Y2O3 additiveinhibit the grain growth of the specimens, but the porosity increases with the increase of Y2O3 content.The optimum optical properties are obtained for the specimens sintered at 1800℃. The grain size increases and the porosity decreases with prolonging the sintering holding time.

     

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