快淬速度对(Nd,Pr)10.5(FeCoZr)83.5B6显微结构和磁性能的影响

Effect of quenching rates on microstructure and magnetic properties of (Nd,Pr)10.5 (FeCoZr)83.5B6 bonded composite magnets

  • 摘要: 采用部分过快淬加后续晶化退火处理工艺,研究了快淬速度对低稀土含量双相复合(Nd,Pr)10.5(FeCoZr)83.5B6合金显微结构和粘结磁体磁性能的影响。合金快淬转轮线速度为24,26,28和30m·s-1,退火温度655~715℃,退火时间5~20min。快淬速度直接影响条带的显微结构和磁体磁性能。以26m·s-1速度快淬出的条带,快淬态由非晶和微晶混合组成,在700℃经10min晶化处理,可获得平均晶粒尺寸约30nm的均匀、细小显微组织,磁性能也最佳。用3.25wt%环氧树脂粘结的磁体磁性能为:Br=0.703T,Hci=544kA·m-1,Hcb=351kA·m-1,(BH)m=70kJ·m-3

     

    Abstract: By using sub-overquenching and ann ealing methods,the effect of quench ing rates on the microstructure and the magnetic pro perties of(Nd,Pr)10.5 (FeCoZr)83.5 B6 bonded composite magnets with low rare-earths content was investi gated.The melted alloy were spun into ribbons at 24,26,28,30m·s-1 wheel surface speed and then the ribb ons were annealed at 655~715℃ for 5~20min.Spun at 26m·s-1,the as-spun ribbons consist of amorphous phases mixed with fine crystallites.And after crystallization in 700℃for 10min,the ribbons have a finer average grain size(about 30nm on free surface) and a more homogeneous microstructu re.The optimal magnetic properties of bonded magnets reaching Br=0.703T,Hci=544kA·m-1,Hcb=351kA·m-1,(BH) m=70kJ·m-3 were obtained by bonding with 3.25wt%epoxy.

     

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