Abstract:
Using Mg powder and B powder as the main raw materials,MgB
2 superconductors were fabricated under different sintering methods.X-ray diffractometer,scanning electron microscopy,the Archimedes method and the standard four-probe resistivity detection method,et al.were used to investigate the phase composition,the microstructure,the density,the critical current density and so on of MgB
2 samples.It is found that the density of MgB
2 bulk decreases with the Mg particle size increasing.The rapidly sintered MgB
2 bulks possess lower density and more non-superconducting phases,such as Mg and MgB
x(x = 4,6 or 12) than the conventionally sintered ones.The rapidly sintered MgB
2 wires exhibit lower critical current density than those conventionally sintered wires.It is revealed that the rapidly sintering method is unfit for the fabrication of high performance MgB
2 superconductors.